Problem with isexychat - Professor and student dating
The second pair of subsamples was treated with a commercial detergent (1.5% SDS), distilled water, 0.1% HCL and another detergent (1.5% triton X-100); they were then submitted to a Soxhlet extraction with ethanol for 60 min and washed with distilled water at 70° C in an ultrasonic bath (method b).The Oxford group divided the precleaned sample into three.
The three control samples, the approximate ages of which were made known to the laboratories, are listed below. T/32) from a tomb excavated at Qasr Ibrîm in Nubia by Professor J. This linen was dated in the British Museum Research Laboratory using liquid scintillation counting, giving a radiocarbon age of 2,010 ± 80 yr BP (BM-2558).
Two were in the form of whole pieces of cloth (samples 2 and 3) and one was in the form of threads (sample 4). This corresponds to a calendar age, rounded to the nearest 5 years, of 110 cal BC - AD 75 cal at the 68 per cent confidence level (where cal denotes calibrated radiocarbon dates). Threads removed from the cope of St Louis d'Anjou which is held in a chapel in the Basilica of Saint-Maximin, Var, France.
Even for the first investigation, there was a possibility of using radiocarbon dating to determine the age of the linen from which the shroud was woven.
The size of the sample then required, however, was ~500cm, which would clearly have resulted in an unacceptable amount of damage, and it was not until the development in the 1970s of small gas-counters and accelerator-mass-spectrometry techniques (AMS), requiring samples of only a few square centimetres, that radiocarbon dating of the shroud became a real possibility. The shroud was separated from the backing cloth along its bottom left-hand edge and a strip (~10 mm x 70 mm) was cut from just above the place where a sample was previously removed in 1973 for examination.
Zurich precleaned the sample in an ultrasonic bath.